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    Dual effectiveness of freezing-thawing and sulfate attack on high-volume slag-incorporated ECC
    (Elsevier Sci Ltd, 2013) Ozbay, Erdogan; Karahan, Okan; Lachemi, Mohamed; Hossain, Khandaker M. A.; Atis, Cengiz Duran
    This study investigated the dual effect of freeze-thaw cycles with sodium sulfate solution on the performance of non-air-entrained Engineering Cementitious Composites (ECCs) with high volumes of slag. ECC specimens containing three different levels of slag content as a replacement for cement (55%, 69% and 81% by weight of total cementitious material) were exposed to aggressive sodium sulfate solution under freezing-thawing cycles. The load-deflection response associated with ultimate mid-span deflection and flexural strength/stiffness was determined, along with crack development behavior. For comparison purposes, the freezing-thawing resistance (in water) of control ECC specimens was also evaluated. Modified point count method air-void parameters, compressive strength, porosity, water absorption and sorptivity tests were also conducted on the virgin ECC specimens (those not exposed to freezing-thawing cycles in water or aggressive sodium sulfate solution). The test results for the virgin specimens revealed that increased slag content (S/PC) improved the ductility, hardened air content, water absorption, porosity and sorptivity of ECC, while marginally decreasing the compressive and flexural strengths. Freeze-thaw cycles in water or sodium sulfate solution showed that the ductility of ECC specimens decreased remarkably, irrespective of slag content and applied freezing-thawing process. Reduction in mass loss was at minimal levels and no significant behavior change was monitored between the specimens undergoing freeze-thaw cycling in water and the aggressive sodium sulfate solution. Moreover, the decrease in flexural stiffness was more evident than the reduction of the flexural strength for all ECC mixtures. Crown Copyright (c) 2012 Published by Elsevier Ltd. All rights reserved.
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    Influence of activator on the strength and drying shrinkage of alkali-activated slag mortar
    (Elsevier Sci Ltd, 2009) Atis, Cengiz Duran; Bilim, Cahit; Celik, Oezlem; Karahan, Okan
    The development of new binders, as an alternative to traditional cement, by the alkaline activation of industrial by-products (i.e. ground granulated slag and fly ash) is an ongoing research topic in the scientific community [Puertas F, Amat T, Jimenez AF, Vazquez T. Mechanical and durable behaviour of alkaline cement mortars reinforced with polypropylene fibres. Cem Concr Res 2003; 33(12): 2031-6]. The aim of this study was to investigate the feasibility of using and alkaline activated ground Turkish slag to produce a mortar without Portland cement (PC). Following the characterization of the slag, mortar specimens made with alkali-activated slag were prepared. Three different activators were used: liquid sodium silicate (LSS), sodium hydroxide (SH) and sodium carbonate (SC) at different sodium concentrations. Compressive and flexural tensile strength of alkali-activated slag mortar was measured at 7-days, 28-days and 3-months. Drying shrinkage of the mortar was measured up to 6-months. Setting times of the alkali-activated slag paste and PC paste were also measured. Setting times of LSS and SH activated slag pastes were found to be much slower than the setting time of PC paste. However, slag paste activated with SC showed similar setting properties to PC paste. LSS, SH and SC activated slag mortar developed 81, 29, and 36 MPa maximum compressive strengths, and 6.8, 3.8, and 5.3 MPa maximum flexural tensile strengths at 28-days. PC mortar developed 33 MPa compressive strength and 5.2 MPa flexural tensile strength. LSS and SH activated slag mortars were found to be more brittle than SC activated slag and PC mortars. Slag mortar made with LSS had a high drying shrinkage, up to six times that of PC mortar. Similarly, slag mortar made with SH had a shrinkage up to three times that of PC mortar. However, SC activated slag mortar had a lower or comparable shrinkage to PC mortar. Therefore, the use of SC as an activator for slag mortar is recommended, since it results in adequate strength, similar setting times to PC mortar and comparable or lower shrinkage. (C) 2007 Elsevier Ltd. All rights reserved.