Effects of ZnO addition on mechanical properties of Bi1.84Pb0.34Sr1.91Ca2.03Cu3.06O10 prepared by a wet technique

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Küçük Resim

Tarih

2009

Dergi Başlığı

Dergi ISSN

Cilt Başlığı

Yayıncı

Elsevier Science Sa

Erişim Hakkı

info:eu-repo/semantics/closedAccess

Özet

In this study, ZnO molar wt% 0, 5,10,20,30, and 50 added Bi1.84Pb0.34Sr1.91Ca2.03Cu3.06O10 superconductors were prepared by wet technique. The experimental works consist of powder X-ray diffraction (XRD) for phase analyses and c-axes parameters, scanning electron microscopy (SEM) for microstructure examination, and microhardness measurements for mechanical properties. These measurements showed that Zn-added material, in comparison with the pure sample, had increased c-axes parameters and decreased grain size. In addition, the experimental results of microhardness measurements were analyzed using Oliver-Pharr model. It was observed that the change of indentation hardness (H-rr) and reduced elastic modulus (E-r) values showed an increasing trend with ZnO addition and exhibited peak load dependence (i.e., indentation size effect (ISE)). (C) 2008 Elsevier B.V. All rights reserved.

Açıklama

Anahtar Kelimeler

Bi-2223, Wet technique, ZnO, Mechanical properties, Depth Sensing Indentation

Kaynak

Journal of Alloys and Compounds

WoS Q Değeri

Q1

Scopus Q Değeri

Q1

Cilt

476

Sayı

1-2

Künye