Optimization of synthesis conditions of PbS thin films grown by chemical bath deposition using response surface methodology

Basit Öğe Kaydı
dc.authoridYucel, Yasin/0000-0002-8572-4213
dc.contributor.authorYucel, Ersin
dc.contributor.authorYucel, Yasin
dc.contributor.authorBeleli, Buse
dc.date.accessioned2024-09-18T20:55:46Z
dc.date.available2024-09-18T20:55:46Z
dc.date.issued2015
dc.departmentHatay Mustafa Kemal Üniversitesien_US
dc.description.abstractIn this study, PbS thin films were synthesized by chemical bath deposition (CBD) under different deposition parameters. Response surface methodology (RSM) was used to optimize synthesis parameters including amount of tri-sodium citrate (0.2-0.8 mL), deposition time (14-34 h) and deposition temperature (26.6-43.4 degrees C) for deposition of the films. 5-level-3-factor central composite design (CCD) was employed to evaluate effects of the deposition parameters on the response (optical band gap of the films). The significant level of both the main effects and the interaction are investigated by analysis of variance (ANOVA). The film structures were characterized by X-ray diffractometer (XRD). Morphological properties of the films were studied with a scanning electron microscopy (SEM). The optical properties of the films were investigated using a UV-visible spectrophotometer. The optimum amount of tri-sodium citrate, deposition time and deposition temperature were found to be 0.7 mL, 18.07 h and 30 degrees C respectively. Under these conditions, the experimental band gap of PbS was 2.20 eV, which is quite good correlation with value (1.98 eV) predicted by the model. (C) 2015 Elsevier B.V. All rights reserved.en_US
dc.identifier.doi10.1016/j.jallcom.2015.03.267
dc.identifier.endpage69en_US
dc.identifier.issn0925-8388
dc.identifier.issn1873-4669
dc.identifier.scopus2-s2.0-84929485023en_US
dc.identifier.scopusqualityQ1en_US
dc.identifier.startpage63en_US
dc.identifier.urihttps://doi.org/10.1016/j.jallcom.2015.03.267
dc.identifier.urihttps://hdl.handle.net/20.500.12483/12043
dc.identifier.volume642en_US
dc.identifier.wosWOS:000354577300010en_US
dc.identifier.wosqualityQ1en_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakScopusen_US
dc.language.isoenen_US
dc.publisherElsevier Science Saen_US
dc.relation.ispartofJournal of Alloys and Compoundsen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectResponse surface methodologyen_US
dc.subjectChemical bath depositionen_US
dc.subjectPbS thin filmsen_US
dc.subjectOptimizationen_US
dc.titleOptimization of synthesis conditions of PbS thin films grown by chemical bath deposition using response surface methodologyen_US
dc.typeArticleen_US

Dosyalar

Orijinal paket
Listeleniyor 1 - 1 / 1
[ N/A ]
İsim:
Tam Metin / Full Text
Boyut:
1.34 MB
Biçim:
Adobe Portable Document Format
İndir

Koleksiyon

WoS İndeksli Yayınlar Koleksiyonu
Scopus İndeksli Yayınlar Koleksiyonu