Elution Conditions for Effective Separation on an Aged Sulfonated Polystyrene-Divinylbenzene (SPD) Column of Organic Acids from Meat

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dc.authoridDURSUN, AHMET/0000-0003-0736-8740
dc.contributor.authorDursun, Ahmet
dc.contributor.authorGueler, Zehra
dc.date.accessioned2024-09-18T20:55:46Z
dc.date.available2024-09-18T20:55:46Z
dc.date.issued2023
dc.departmentHatay Mustafa Kemal Üniversitesien_US
dc.description.abstractA modified elution condition for organic acids in meat chromatographed by aged sulfonated polystyrene-divinylbenzene (SPD) column was compared to common elution conditions in terms of efficiency, selectivity, resolution, peak shape, precision, and accuracy. The mobile phase concentration (mM), flow rate (mL/min), and column temperature (?) under common elution conditions (CECs) changed from 10 to 25, 0.6 to 0.2, and 60 to 40 in modified elution (MEC), respectively. A total of 15 peaks were detected in both elution conditions. Seven of them were confirmed with the available authentic organic acid standards including citric, pyruvic, succinic, lactic, acetic, propionic, and butyric acid. A good efficiency, selectivity, resolution, and peak shape were obtained for organic acids chromatographed on aged SPD column with MEC compared to CEC. The analyte was quantified using external standard technique. High response factor, expected correction factor, better calibration sensitivity and repeatability, and also accuracy for organic acids were observed under MEC. In particular, when peak broadening was observed in the aged SPD column, good chromatographic separation could be obtained with MEC in terms of resolution and peak shape was associated with better precision and recovery for organic acids in meat.en_US
dc.identifier.doi10.1007/s12161-023-02448-x
dc.identifier.endpage708en_US
dc.identifier.issn1936-9751
dc.identifier.issn1936-976X
dc.identifier.issue4en_US
dc.identifier.scopus2-s2.0-85146576598en_US
dc.identifier.scopusqualityQ1en_US
dc.identifier.startpage699en_US
dc.identifier.urihttps://doi.org/10.1007/s12161-023-02448-x
dc.identifier.urihttps://hdl.handle.net/20.500.12483/12042
dc.identifier.volume16en_US
dc.identifier.wosWOS:000918684300001en_US
dc.identifier.wosqualityQ2en_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakScopusen_US
dc.language.isoenen_US
dc.publisherSpringeren_US
dc.relation.ispartofFood Analytical Methodsen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectResponse factoren_US
dc.subjectResolutionen_US
dc.subjectPeak shapeen_US
dc.subjectRecoveryen_US
dc.subjectOrganic aciden_US
dc.titleElution Conditions for Effective Separation on an Aged Sulfonated Polystyrene-Divinylbenzene (SPD) Column of Organic Acids from Meaten_US
dc.typeArticleen_US

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