Spectral Classical Least Square Calibration Approach for the Simultaneous Determination and Stability Test of Sulphadiazine and Trimethoprim in Bolus

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dc.contributor.authorEge, Hismiogullari Sahver
dc.contributor.authorEnder, Yarsan
dc.contributor.authorDinc, Erdal
dc.date.accessioned2024-09-18T20:59:04Z
dc.date.available2024-09-18T20:59:04Z
dc.date.issued2010
dc.departmentHatay Mustafa Kemal Ãœniversitesien_US
dc.description.abstractA simple spectral classical least square calibration approach were proposed for the simultaneous quantitative evaluation and stability testing of sulphadiazine and trimethoprim in an animal commercial preparation, bolus without requiring a priory separation step. Stability tests of sulphadiazine and trimethoprim in bolus were performed by using the following conditions: Room temperature, refrigerator and etuve (37 degrees C) for each 3 month during 12 months. A spectral classical least square calibration based on the use of absorptivities at three-wavelength set (241, 257 and 288 nm) was computed by using the linear concentration range of 4.0-22.0 mu g mL(-1) for sulphadiazine and 3.0-18.0 mu g mL(-1) for trimethoprim. The proposed spectral least square calibration was validated by using various synthetic binary mixtures containing the above veterinary drugs. Simultaneous analysis and stability test of sulphadiazine and trimethoprim in commercial veterinary bolus was established by the spectral classical calibration method.en_US
dc.identifier.endpage861en_US
dc.identifier.issn1680-5593
dc.identifier.issn1993-601X
dc.identifier.issue4en_US
dc.identifier.startpage857en_US
dc.identifier.urihttps://hdl.handle.net/20.500.12483/12338
dc.identifier.volume9en_US
dc.identifier.wosWOS:000275982800041en_US
dc.identifier.wosqualityQ3en_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.language.isoenen_US
dc.publisherMedwell Onlineen_US
dc.relation.ispartofJournal of Animal and Veterinary Advancesen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/openAccessen_US
dc.subjectSpectral classical least squareen_US
dc.subjectsimultaneous determinationen_US
dc.subjectstability testen_US
dc.subjectsulphadiazineen_US
dc.subjecttrimethoprimen_US
dc.subjectchemometryen_US
dc.titleSpectral Classical Least Square Calibration Approach for the Simultaneous Determination and Stability Test of Sulphadiazine and Trimethoprim in Bolusen_US
dc.typeArticleen_US

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