Electrochemical synthesis of poly(pyrrole-co-o-anisidine)/chitosan composite films
dc.contributor.author | Yalcinkaya, Suleyman | |
dc.contributor.author | Cakmak, Didem | |
dc.date.accessioned | 2024-09-18T20:55:34Z | |
dc.date.available | 2024-09-18T20:55:34Z | |
dc.date.issued | 2017 | |
dc.department | Hatay Mustafa Kemal Üniversitesi | en_US |
dc.description.abstract | In this study, poly(pyrrole-co-o-anisidine)/chitosan composite films were electrochemically synthesized in various monomers feed ratio (pyrrole: o-anisidine; 9:1, 7:3,1:1, 3:7 and 1:9) of pyrrole and o-anisidine on the platinum electrode. Electrochemical synthesis of the composite films was carried out via cyclic voltammetry technique. They were characterized by FT-IR, cyclic voltammetry, SEM micrographs, digital images, TGA and DSC techniques. The SEM results indicated that the particle size of the composite decreased with increasing o-anisidine ratio and the films became more likely to be smooth morphology. The TGA results proved that the film of the composite with 1:1 ratio showed highest final degradation temperature and lowest weight loss (83%) compared to copolymer and 9:1 1:9 composite films. The 1:1 composite film had higher thermal stability than copolymer and the other composite films (9:1 1:9). Meanwhile, electrochemical studies exhibited that the 1/9 composite film had good electrochemical stability as well. (C) 2017 Elsevier B.V. All rights reserved. | en_US |
dc.description.sponsorship | Scientific and Technological Research Council of Turkey (TUBITAK) [112T523] | en_US |
dc.description.sponsorship | This study has been supported by the Scientific and Technological Research Council of Turkey (TUBITAK). (Project number: 112T523). | en_US |
dc.identifier.doi | 10.1016/j.molstruc.2017.01.040 | |
dc.identifier.endpage | 43 | en_US |
dc.identifier.issn | 0022-2860 | |
dc.identifier.issn | 1872-8014 | |
dc.identifier.scopus | 2-s2.0-85009961769 | en_US |
dc.identifier.scopusquality | Q1 | en_US |
dc.identifier.startpage | 32 | en_US |
dc.identifier.uri | https://doi.org/10.1016/j.molstruc.2017.01.040 | |
dc.identifier.uri | https://hdl.handle.net/20.500.12483/11931 | |
dc.identifier.volume | 1135 | en_US |
dc.identifier.wos | WOS:000395604700005 | en_US |
dc.identifier.wosquality | Q3 | en_US |
dc.indekslendigikaynak | Web of Science | en_US |
dc.indekslendigikaynak | Scopus | en_US |
dc.language.iso | en | en_US |
dc.publisher | Elsevier Science Bv | en_US |
dc.relation.ispartof | Journal of Molecular Structure | en_US |
dc.relation.publicationcategory | Makale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı | en_US |
dc.rights | info:eu-repo/semantics/closedAccess | en_US |
dc.subject | Pyrrole | en_US |
dc.subject | o-anisidine | en_US |
dc.subject | Chitosan | en_US |
dc.subject | Composite | en_US |
dc.subject | Electrochemical synthesis | en_US |
dc.title | Electrochemical synthesis of poly(pyrrole-co-o-anisidine)/chitosan composite films | en_US |
dc.type | Article | en_US |
Dosyalar
Orijinal paket
1 - 1 / 1