Synthesis, characterization, swelling behavior and metal uptake studies of dichloroglyoxime crosslinked chitosan derivative

dc.authorid0000-0001-5914-607Xen_US
dc.contributor.authorTimur, Mahir
dc.date.accessioned2020-09-04T11:06:53Z
dc.date.available2020-09-04T11:06:53Z
dc.date.issued2019en_US
dc.departmentAltınözü Tarım Bilimleri Meslek Yüksekokuluen_US
dc.description.abstractNew crosslinked derivative of chitosan was prepared by the condensation reaction of chitosan (CS) and dichloro glyoxime. Structural analysis of chitosan derivative (CSL) was performed by elemental analysis (C, H, N), SEM measurements, FT-IR, solid-state 13C CP/MAS NMR, XRD-powder and TGA. Crosslinking ratio was determined from the elemental analysis by using the C/N and found to be 70%. The swelling behavior of derivative was investigated on pH 3-7 and 10 at 25 and 37°C. Metal ion uptake capacity was studied towards of selected transition metals Cu(II), Ni(II), Co(II), Fe(II) and (Cd(II) cations in aqueous medium. According to the results of the analyses; water retention capacity and metal uptake capacity of new cross-linked chitosan derivative is higher than chitosan and metal uptake sequence are Cu(II) > Fe(II) >Cd(II) > Co(II) > Ni(II) respectively.en_US
dc.identifier.citationTimur, M. (2019). Synthesis, Characterization, Swelling Behavior and Metal Uptake Studies of Dichloroglyoxime Crosslinked Chitosan Derivative. Hittite Journal of Science & Engineering, 6(1), 37-44.en_US
dc.identifier.doi10.17350/HJSE19030000131en_US
dc.identifier.endpage44en_US
dc.identifier.issn2149-2123
dc.identifier.issn2148-4171
dc.identifier.issue1en_US
dc.identifier.startpage37en_US
dc.identifier.trdizinid337928en_US
dc.identifier.urihttps://dx.doi.org/10.17350/HJSE19030000131
dc.identifier.urihttps://hdl.handle.net/20.500.12483/3036
dc.identifier.volume6en_US
dc.indekslendigikaynakTR-Dizinen_US
dc.language.isoenen_US
dc.publisherHitit Üniversitesien_US
dc.relation.ispartofHittite Journal of Science and Engineeringen_US
dc.relation.publicationcategoryMakale - Ulusal Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/openAccessen_US
dc.rightsAttribution-NonCommercial 3.0 United States*
dc.rights.urihttp://creativecommons.org/licenses/by-nc/3.0/us/*
dc.subjectCrosslinken_US
dc.subjectChitosanen_US
dc.subjectSwellingen_US
dc.subjectMetal-ion uptakeen_US
dc.titleSynthesis, characterization, swelling behavior and metal uptake studies of dichloroglyoxime crosslinked chitosan derivativeen_US
dc.typeArticleen_US

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